T-cut slotted quartz tube-atom trap strategy for the on-line preconcentration of thallium in well water samples

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dc.authorid0000-0003-0745-6863en_US
dc.authorscopusid57215201333en_US
dc.authorwosidDRB-8392-2022en_US
dc.contributor.authorBombom, Miray
dc.contributor.authorZaman, Buse Tuğba
dc.contributor.authorDalgıç Bozyiğit, Gamze
dc.contributor.authorŞaylan, Meltem
dc.contributor.authorBayraktar, Ahsen
dc.contributor.authorArvas, Büşra
dc.contributor.authorYolaçan, Çiğdem
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2023-08-01T06:21:00Z
dc.date.available2023-08-01T06:21:00Z
dc.date.issued2023en_US
dc.departmentFakülteler, Eczacılık Fakültesi, Eczacılık Meslek Bilimleri Bölümü, Analitik Kimya Ana Bilim Dalıen_US
dc.description.abstractIn this study, an on-line preconcentration system was developed for the quantitative determination of thallium in well water samples using hydrogen-assisted T-cut slotted quartz tube atom trapping (HA-T-SQT-AT) coupled to flame atomic absorption spectrometry (FAAS). The method is based on trapping the thallium atoms on the inner surface of the T-SQT for a short period using sample aspiration and lean flame conditions. Then, hydrogen gas as a reducing agent was released instantly to free the trapped analyte atoms, resulting in a sharp and narrow signal. The system analytical performance was enhanced by performing comprehensive optimization of several factors. The linear range and LOD/LOQ values of the optimized method were found to be 7.5–––200 ng/mL and 2.6/8.7 ng/mL, respectively. Accuracy/practicability of the presented method were verified using well water samples, and the percent recoveries calculated using the external calibration approach were all above 80%.en_US
dc.identifier.citationBombom, M., Zaman, B. T., Dalgıç Bozyiğit, G., Şaylan, M., Bayraktar, A., Arvas, B., Yolaçan, Ç., & Bakırdere, S. (2023). T-cut slotted quartz tube-atom trap strategy for the on-line preconcentration of thallium in well water samples. Measurement, 220, pp. 1-7. https://doi.org/10.1016/j.measurement.2023.113363en_US
dc.identifier.doi10.1016/j.measurement.2023.113363en_US
dc.identifier.endpage7en_US
dc.identifier.issn1873-412X
dc.identifier.issn0263-2241
dc.identifier.scopus2-s2.0-85165542060en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://hdl.handle.net/20.500.13055/516
dc.identifier.urihttps://doi.org/10.1016/j.measurement.2023.113363
dc.identifier.volume220en_US
dc.identifier.wosWOS:001048966200001en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorŞaylan, Meltem
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofMeasurementen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.relation.tubitakinfo:eu-repo/grantAgreement/TUBITAK/SOBAG/1919B012100881
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectThalliumen_US
dc.subjectFlame Atomic Absorption Spectrometryen_US
dc.subjectAtom Trapen_US
dc.subjectT-Shaped Slotted Quartz Tubeen_US
dc.subjectWell Wateren_US
dc.titleT-cut slotted quartz tube-atom trap strategy for the on-line preconcentration of thallium in well water samplesen_US
dc.typeArticleen_US
dspace.entity.typePublication

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