Microwave assisted effective synthesis of CdS nanoparticles to determine the copper ions in artichoke leaves extract samples by flame atomic absorption spectrometry

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dc.authorscopusid57215201333en_US
dc.authorwosidDRB-8392-2022en_US
dc.contributor.authorŞaylan, Meltem
dc.contributor.authorMetin, Berfin
dc.contributor.authorAkbıyık, Hilal
dc.contributor.authorTurak, Fatma
dc.contributor.authorÇetin, Gülten
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2022-11-11T08:06:21Z
dc.date.available2022-11-11T08:06:21Z
dc.date.issued2023en_US
dc.departmentFakülteler, Eczacılık Fakültesi, Eczacılık Meslek Bilimleri Bölümü, Analitik Kimya Ana Bilim Dalıen_US
dc.description.abstractIn this study, an accurate and sensitive analytical strategy based on cadmium sulfide nanoparticles assisted dispersive solid phase extraction (CdS-NPs-DSPE) was developed for the preconcentration/separation of copper ions in the extract of artichoke leaves. The CdS-NPs-DSPE method was combined with slotted quartz tube-flame atomic absorption spectrometry (SQT-FAAS) for the first time. The CdS-NPs were synthesized using microwave-assisted reaction as a new and rapid synthesis method for the CdS precursor solution. The morphology and structure of the synthesized sorbent were characterized using SEM, XRD, and FT-IR. The optimum conditions of the method were as follows: 40 mL sample volume, 0.10 mL of pH 4.0 buffer solution, 7.5 mg CdS NPs, 30 s sonication period, and 100 µL of concentrated HNO3. According to the experimental results, the calibration plot was linear in the concentration range of 2.5–30 µg/L, with a detection limit of 0.71 µg/L. The enhancement in detection power was calculated as 162-folds based on LOD comparison. The reliability and applicability of the proposed method were validated by spiking artichoke leave extracts at different concentrations. The percent recoveries calculated for 50 and 150 µg/L piked samples were 87 ± 12.6 % and 116.8 ± 3.2 %, respectively. These findings verify that the proposed method can be used for accurate and precise determination of copper ions in artichoke leaves.en_US
dc.identifier.citationŞaylan, M., Metin, B., Akbıyık, H., Turak, F., Çetin, G. & Bakırdere, S. (2022). Microwave assisted effective synthesis of CdS nanoparticles to determine the copper ions in artichoke leaves extract samples by flame atomic absorption spectrometry. Journal of Food Composition and Analysis, 155, pp. 1-7. https://doi.org/10.1016/j.jfca.2022.104965en_US
dc.identifier.doi10.1016/j.jfca.2022.104965en_US
dc.identifier.endpage7en_US
dc.identifier.issn0889-1575
dc.identifier.scopus2-s2.0-85139835003en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1016/j.jfca.2022.104965
dc.identifier.urihttps://hdl.handle.net/20.500.13055/305
dc.identifier.volume115en_US
dc.identifier.wosWOS:000888172400004en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorŞaylan, Meltem
dc.language.isoenen_US
dc.publisherAcademic Press Inc.en_US
dc.relation.ispartofJournal of Food Composition and Analysisen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectArtichoke Leavesen_US
dc.subjectCadmium Sulfide Nanoparticlesen_US
dc.subjectCopperen_US
dc.subjectDispersive Solid Phase Extractionen_US
dc.subjectFlame Atomic Absorption Spectrometryen_US
dc.titleMicrowave assisted effective synthesis of CdS nanoparticles to determine the copper ions in artichoke leaves extract samples by flame atomic absorption spectrometryen_US
dc.typeArticleen_US
dspace.entity.typePublication

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