CoSn(OH)6 nanocubes as a solid sorbent for the effective preconcentration of copper ions in cinnamon (Cinnamomum zeylanicum) extract

dc.authorid0000-0003-0745-6863en_US
dc.authorscopusid57215201333en_US
dc.authorwosidDRB-8392-2022en_US
dc.contributor.authorBahçıvan, Aleyna
dc.contributor.authorŞaylan, Meltem
dc.contributor.authorSağdıç, Osman
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2024-03-25T08:47:40Z
dc.date.available2024-03-25T08:47:40Z
dc.date.issued2024en_US
dc.departmentFakülteler, Eczacılık Fakültesi, Eczacılık Meslek Bilimleri Bölümü, Analitik Kimya Ana Bilim Dalıen_US
dc.description.abstractThis study was aimed at developing a simple and efficient CoSn(OH)6 nanocubes-based preconcentration method for the preconcentration of copper ions from cinnamon extracts for determination by flame atomic absorption spectrometry. The cube-shaped sorbent was synthesized using the simple stoichiometric co-precipitation method under ambient conditions. Experimental factors of the method were evaluated with a comprehensive optimization approach to maximize the extraction efficiency for the analyte. Under the optimal conditions, the limit of detection (LOD), limit of quantitation (LOQ), and linear dynamic range were recorded as 0.98 µg/L, 3.28 µg/L, and 4.0-75 µg/L, respectively. The enhancement factor was calculated as 101.6-fold by comparing the LODs of the optimized and direct analysis systems. Percent recoveries were found to be within an acceptable range (77.6-115 %), with high repeatability using matrix matching calibration strategy. Results validated the proposed method as a highly efficient extraction approach for the monitoring of copper ions in herbal cinnamon extracts.en_US
dc.identifier.citationBahçıvan, A., Şaylan, M., Sağdıç, O., & Bakırdere, S. (2024). CoSn(OH)6 nanocubes as a solid sorbent for the effective preconcentration of copper ions in cinnamon (Cinnamomum zeylanicum) extract. Food Chemistry, 447, pp. 1-7. https://doi.org/10.1016/j.foodchem.2024.139037en_US
dc.identifier.doi10.1016/j.foodchem.2024.139037en_US
dc.identifier.endpage7en_US
dc.identifier.issn0308-8146
dc.identifier.issn1873-7072
dc.identifier.pmidPMID: 38513484en_US
dc.identifier.scopus2-s2.0-85188240000en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1016/j.foodchem.2024.139037
dc.identifier.urihttps://hdl.handle.net/20.500.13055/679
dc.identifier.volume447en_US
dc.identifier.wosWOS:001221922700001en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorŞaylan, Meltem
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofFood Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCopperen_US
dc.subjectCube-Shaped Nanomaterialen_US
dc.subjectFlame Atomic Absorption Spectrometryen_US
dc.subjectHerbal Extracten_US
dc.subjectMatrix Matching Calibrationen_US
dc.titleCoSn(OH)6 nanocubes as a solid sorbent for the effective preconcentration of copper ions in cinnamon (Cinnamomum zeylanicum) extracten_US
dc.typeArticleen_US
dspace.entity.typePublication

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Kapalı Erişim
İsim:
CoSn(OH)6 nanocubes as a solid sorbent for the effective preconcentration of copper ions in cinnamon (Cinnamomum zeylanicum) extract.pdf
Boyut:
1.38 MB
Biçim:
Adobe Portable Document Format
Açıklama:
Tam Metin / Full Text
Lisans paketi
Listeleniyor 1 - 1 / 1
Kapalı Erişim
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama: