Plastic sieve equipped two-syringe assisted magnetic colloidal gel for dispersive solid-phase extraction of manganese in tea samples

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dc.authorid0000-0003-2303-0408en_US
dc.authoridQ1en_US
dc.authoridQ1en_US
dc.authorscopusid57190251193en_US
dc.contributor.authorAydın, Efe Sinan
dc.contributor.authorZaman, ‪Buse Tuğba
dc.contributor.authorSerbest, Hakan
dc.contributor.authorKapukıran, Fatih
dc.contributor.authorTurak, Fatma
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2022-10-06T08:50:31Z
dc.date.available2022-10-06T08:50:31Z
dc.date.issued2022en_US
dc.departmentFakülteler, Mühendislik ve Doğa Bilimleri Fakültesi, Kimya Mühendisliği Bölümüen_US
dc.description.abstractIn this study, a simple and effective analytical method was described for the determination of manganese in a spectrometric system. For this purpose, a plastic sieve fitted between two syringes was used as a dispersive solid phase extraction tool. The extraction of manganese was performed by using a magnetic colloidal gel (MCG), which was formed by mixing cobalt magnetic nanoparticle (Co-MNP) and deep eutectic solvent. All experimental parameters of the method including Co-MNP amount in MCG, MCG volume, cycle number for pressurized mixing in the two-syringe system and eluent type/volume in the desorption step were carefully evaluated in order to find the best experimental conditions for efficient extraction/preconcentration of manganese. The detection limit was calculated as 4.0 ng/mL for manganese extracted by 150 µL of MCG from 8.0 mL of aqueous solution at pH 10 with 8 cycles of pressurized mixing. In order to validate the applicability and the accuracy of the developed system, the optimum conditions were applied to jasmine tea samples. The tea samples were analyzed using the standard addition method and the manganese the manganese content were found in the range of 133 – 245 ng/mL. The obtained results showed that the developed method is applicable, accurate and feasible for the determination of manganese at trace levels.en_US
dc.identifier.citationAydin, E. S., Zaman, B. T., Serbest, H., Kapukiran, F., Turak, F., & Bakirdere, S. (2022). Plastic sieve equipped two-syringe assisted magnetic colloidal gel for dispersive solid-phase extraction of manganese in tea samples. Journal of Food Composition and Analysis, 114, 1-7. https://doi.org/10.1016/j.jfca.2022.104833en_US
dc.identifier.doi10.1016/j.jfca.2022.104833en_US
dc.identifier.endpage7en_US
dc.identifier.issn0889-1575
dc.identifier.scopus2-s2.0-85136561942en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1016/j.jfca.2022.104833
dc.identifier.urihttps://hdl.handle.net/20.500.13055/279
dc.identifier.volume114en_US
dc.identifier.wosWOS:000863108700013en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorSerbest, Hakan
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofJournal of Food Composition and Analysisen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectManganeseen_US
dc.subjectPlastic sieveen_US
dc.subjectSlotted quartz tubeen_US
dc.subjectDispersive solid phase extractionen_US
dc.subjectMagnetic colloidal gelen_US
dc.subjectJasmine teaen_US
dc.titlePlastic sieve equipped two-syringe assisted magnetic colloidal gel for dispersive solid-phase extraction of manganese in tea samplesen_US
dc.typeArticleen_US
dspace.entity.typePublication

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