Nickel hydroxide nanoflower-based dispersive solid-phase extraction of copper from water matrix

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dc.authorscopusid57215201333en_US
dc.contributor.authorŞaylan, Meltem
dc.contributor.authorDemirel, Rabia
dc.contributor.authorFırat Ayyıldız, Merve
dc.contributor.authorChormey, Doste Selali
dc.contributor.authorÇetin, Gülten
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2022-11-24T06:29:39Z
dc.date.available2022-11-24T06:29:39Z
dc.date.issued2023en_US
dc.departmentFakülteler, Eczacılık Fakültesi, Eczacılık Meslek Bilimleri Bölümü, Analitik Kimya Ana Bilim Dalıen_US
dc.descriptionYıldız Technical University -- FBA-2021–4725en_US
dc.description.abstractIn this work, a dispersive solid-phase extraction method based on Ni(OH)2 nanoflowers (Ni(OH)2-NFs-DSPE) was developed to separate and preconcentrate copper ions from tap water samples for determination by flame atomic absorption spectrometry (FAAS). Ni(OH)2-NFs was synthesized using a homogeneous precipitation technique and used as sorbent for copper preconcentration. X-ray diffraction, scanning electron microscopy, and Fourier-transform infrared spectroscopy were used to characterize the synthesized sorbent. All experimental variables were carefully optimized to achieve a high enhancement factor of 107.5-folds with respect to the detection sensitivity of the conventional FAAS. The proposed method's analytical parameters including LOD, LOQ, and linear range were determined as 1.33 μg/L, 4.42 μg/L, and 3.0-40 μg/L, respectively. To assess the applicability and reliability of the developed method, optimal conditions were applied to tap water samples and satisfactory percent recoveries (94-103%) were obtained for the samples spiked at 20 and 30 μg/L. This validated the accuracy and feasibility of the developed method to real samples. The developed method can be described as a simple, efficient, and rapid analytical approach for the accurate determination of trace copper ions in water samples.en_US
dc.identifier.citationŞaylan, M., Demirel, R., Fırat Ayyıldız, M., Chormey, D. S., Çetin, G. & Bakırdere, S. (2023). Nickel hydroxide nanoflower-based dispersive solid-phase extraction of copper from water matrix. Environmental Monitoring and Assessment, 195(1), pp. 1-11. https://doi.org/10.1007/s10661-022-10653-0en_US
dc.identifier.doi10.1007/s10661-022-10653-0en_US
dc.identifier.endpage11en_US
dc.identifier.issn0167-6369
dc.identifier.issn1573-2959
dc.identifier.issue1en_US
dc.identifier.pmidPMID: 36409393en_US
dc.identifier.scopus2-s2.0-85142262364en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1007/s10661-022-10653-0
dc.identifier.urihttps://hdl.handle.net/20.500.13055/318
dc.identifier.volume195en_US
dc.identifier.wosWOS:000886210600004en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynakPubMeden_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorŞaylan, Meltem
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofEnvironmental Monitoring and Assessmenten_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCopperen_US
dc.subjectNi(OH)2 Nanoflowersen_US
dc.subjectDispersive Solid-Phase Extractionen_US
dc.subjectFlame Atomic Absorption Spectrometryen_US
dc.subjectTap Wateren_US
dc.titleNickel hydroxide nanoflower-based dispersive solid-phase extraction of copper from water matrixen_US
dc.typeArticleen_US
dspace.entity.typePublication

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