Development of analytical strategy for the determination of cadmium by flame atomic absorption spectrometry after dithizone/deep eutectic solvent probe based liquid phase microextraction

Basit Öğe Kaydı
dc.authorid0000-0003-2303-0408
dc.contributor.authorAkbıyık, Hilal
dc.contributor.authorSerbest, Hakan
dc.contributor.authorKılınç, Yağmur
dc.contributor.authorOflu, Sude
dc.contributor.authorGürsoy, Selim
dc.contributor.authorÖzdoğan, Nizamettin
dc.contributor.authorÇetin, Gülten
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2024-09-17T06:58:02Z
dc.date.available2024-09-17T06:58:02Z
dc.date.issued2024
dc.departmentFakülteler, Mühendislik ve Doğa Bilimleri Fakültesi, Kimya Mühendisliği Bölümü
dc.description.abstractLiquid phase microextraction (LPME) with a dithizone/deep eutecticsolvent (DTZ-DES)-based probe was employed for the determinationof trace cadmium by flame atomic absorption spectrometry (FAAS).All extraction parameters were univariately optimized to achieve thehighest efficiency and the limits of detection and quantification were3.5 and 11.8 ng mL−1. Good linearity was obtained from 10 to200 ng mL−1 with a regression coefficient (R2) of 0.9979. The sensitiv-ity of FAAS system was improved 26.9-fold by the microextractionprocedure. The accuracy and applicability of the method were inves-tigated with recovery experiments carried out using corn silk teaextracts. The recovery values with matrix matching calibration werefrom 81.3 to 114.3%, demonstrating that this environmentallyfriendly method is applicable for determination of cadmium in teasamples with good accuracy.
dc.description.sponsorshipYTU Scientific Research Project numbered -- FBA-2022-5035.
dc.identifier.citationAkbıyık, H., Serbest, H., Kılınç, Y., Oflu, S., Gürsoy, S., Özdoğan, N., Çetin, G., & Bakırdere, S. (2024). Development of analytical strategy for the determination of cadmium by flame atomic absorption spectrometry after dithizone/deep eutectic solvent probe based liquid phase microextraction. Analytical Letters, pp. 1-12. https://doi.org/10.1080/00032719.2024.2401172
dc.identifier.doi10.1080/00032719.2024.2401172
dc.identifier.endpage12
dc.identifier.issn0003-2719
dc.identifier.issn1532-236X
dc.identifier.scopus2-s2.0-85204016826
dc.identifier.scopusqualityQ2
dc.identifier.startpage1
dc.identifier.urihttps://doi.org/10.1080/00032719.2024.2401172
dc.identifier.urihttps://hdl.handle.net/20.500.13055/790
dc.identifier.wosWOS:001312584500001
dc.identifier.wosqualityQ3
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expanded
dc.institutionauthorSerbest, Hakan
dc.institutionauthorid0000-0003-2303-0408
dc.language.isoen
dc.publisherTaylor & Francis
dc.relation.ispartofAnalytical Letters
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectCadmium
dc.subjectCorn Silk
dc.subjectDeepeutectic Solvent
dc.subjectDithizone
dc.subjectFlame Atomic Absorptionspectrometry (FAAS)
dc.titleDevelopment of analytical strategy for the determination of cadmium by flame atomic absorption spectrometry after dithizone/deep eutectic solvent probe based liquid phase microextraction
dc.typeArticle
dspace.entity.typePublication

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