Determination of rhodium in soil by DispersiveSolid-Phase Extraction (DSPE) with manganese ferrite nanoparticles and Flame Atomic Absorption Spectrometry(FAAS)

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dc.authorid0000-0003-2303-0408en_US
dc.authorscopusid57190251193en_US
dc.authorwosidCAG-6203-2022en_US
dc.contributor.authorSerbest, Hakan
dc.date.accessioned2023-05-15T13:57:42Z
dc.date.available2023-05-15T13:57:42Z
dc.date.issued2024en_US
dc.departmentFakülteler, Mühendislik ve Doğa Bilimleri Fakültesi, Kimya Mühendisliği Bölümüen_US
dc.description.abstractManganese ferrite (MnFe2O4) nanoparticles-assisted dispersive solid-phase extraction (MF-DSPE) was developed for the determination ofrhodium (Rh) in soil samples at low levels with good accuracy andprecision by flame atomic absorption spectrometry (FAAS). The syn-thesis of MnFe2O4nanoparticles was carried out in a microwave sys-tem by a rapid procedure. The pH, buffer volume, sorbent mass,sample volume, eluent volume/concentration, and mixing time wereidentified with univariate optimization. Under the optimal conditions,the limits of detection (LOD) and quantitation (LOQ) were 4.4 and14.7mgL 1, respectively. The sensitivity was improved by 121.9-foldbased upon comparison of the limits of detection with and withoutpreconcentration. The applicability was investigated by spiking rho-dium into soil extracts, and good recovery results between 91.2%and 122.2% were achieved using matrix matching calibration. Theresults showed that MF-DSPE-FAAS determines low levels of rhodiumin soil with good accuracy and precision.en_US
dc.identifier.citationSerbest, H. (2024). Determination of rhodium in soil by DispersiveSolid-Phase Extraction (DSPE) with manganese ferrite nanoparticles and Flame Atomic Absorption Spectrometry(FAAS). Analytical Letters, 57(3), pp. 456–468. https://doi.org/10.1080/00032719.2023.2212092en_US
dc.identifier.doi10.1080/00032719.2023.2212092en_US
dc.identifier.endpage468en_US
dc.identifier.issn0003-2719
dc.identifier.issn1532-236X
dc.identifier.issue3en_US
dc.identifier.scopus2-s2.0-85159265915en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage456en_US
dc.identifier.urihttps://doi.org/10.1080/00032719.2023.2212092
dc.identifier.urihttps://hdl.handle.net/20.500.13055/465
dc.identifier.volume57en_US
dc.identifier.wosWOS:000985866800001en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorSerbest, Hakan
dc.language.isoenen_US
dc.publisherTaylor & Francisen_US
dc.relation.ispartofAnalytical Lettersen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDispersive Solid-Phase Extraction (DSPE)en_US
dc.subjectFlame Atomic Absorption Spectrometry (FAAS)en_US
dc.subjectManganese Ferrite(MnFe2O4) Nanoparticlesen_US
dc.subjectMicrowave Synthesisen_US
dc.subjectRhodiumen_US
dc.titleDetermination of rhodium in soil by DispersiveSolid-Phase Extraction (DSPE) with manganese ferrite nanoparticles and Flame Atomic Absorption Spectrometry(FAAS)en_US
dc.typeArticleen_US
dspace.entity.typePublication

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