Trace cadmium determination in lake water matrix by flame atomic absorption spectrometry after manganese ferrite magnetic nanoparticles-based dispersive solid phase extraction

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dc.authorid0000-0003-2303-0408en_US
dc.authorscopusid57190251193en_US
dc.authorwosidCAG-6203-2022en_US
dc.contributor.authorKaraman, Devrim Nur
dc.contributor.authorSerbest, Hakan
dc.contributor.authorKılınç, Yağmur
dc.contributor.authorDemirel, Rabia
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2023-07-29T08:23:50Z
dc.date.available2023-07-29T08:23:50Z
dc.date.issued2023en_US
dc.departmentFakülteler, Mühendislik ve Doğa Bilimleri Fakültesi, Kimya Mühendisliği Bölümüen_US
dc.description.abstractIn this study, manganese ferrite magnetic nanoparticles-based dispersive solid phase extraction (MF-MNP-DSPE) was developed for cadmium determination at trace level by flame atomic absorption spectrometry (FAAS). Manganese ferrite-based magnetic nanoparticles were synthesized to be used as solid phase extraction sorbent. All the analytical conditions were optimized by univariate optimization approach to achieve high enrichment factors. Under the optimum conditions, limit of detection (LOD) and quantification (LOQ) values of the developed method were recorded as 1.3 and 4.3 µg L−1, respectively. Approximately 135-fold improvement in the detection power by the MF-MNP-DSPE-FAAS system was recorded over the traditional FAAS system based on LOD comparison. Recovery experiments were performed to test the applicability/accuracy of the developed method with lake water spiked at different concentrations. Percent recovery values were obtained between 87% and 112% by employing the matrix matching calibration strategy and this showed that the developed method is applicable for the determination of cadmium in lake water samples with high accuracy and precision.en_US
dc.identifier.citationKaraman, D. N., Serbest, H., Kılınç, Y., Demirel, R., & Bakırdere, S. (2023). Trace cadmium determination in lake water matrix by flame atomic absorption spectrometry after manganese ferrite magnetic nanoparticles-based dispersive solid phase extraction. Clean - Soil, Air, Water, 51(9), pp. 1-8. https://doi.org/10.1002/clen.202200186en_US
dc.identifier.doi10.1002/clen.202200186en_US
dc.identifier.endpage8en_US
dc.identifier.issue9en_US
dc.identifier.scopus2-s2.0-85165505367en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1002/clen.202200186
dc.identifier.urihttps://hdl.handle.net/20.500.13055/512
dc.identifier.volume51en_US
dc.identifier.wosWOS:001031519500001en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorSerbest, Hakan
dc.language.isoenen_US
dc.publisherWileyen_US
dc.relation.ispartofClean - Soil, Air, Wateren_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectCadmiumen_US
dc.subjectDispersive Solid Phase Extractionen_US
dc.subjectFlame Atomic Absorption Spectrophotometryen_US
dc.subjectMan-Ganese Ferrite Magnetic Nanoparticlesen_US
dc.titleTrace cadmium determination in lake water matrix by flame atomic absorption spectrometry after manganese ferrite magnetic nanoparticles-based dispersive solid phase extractionen_US
dc.typeArticleen_US
dspace.entity.typePublication

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