Development of an analytical strategy for the determination of trace lead in hibiscus tea extract by double slotted quartz tube assisted flame atomic absorption spectrometry after manganese ferrite based dispersive solid phase extraction

Basit Öğe Kaydı
dc.authorid0000-0003-2303-0408en_US
dc.authorscopusid57190251193en_US
dc.authorwosidCAG-6203-2022en_US
dc.contributor.authorKaraman, Devrim Nur
dc.contributor.authorSerbest, Hakan
dc.contributor.authorBahçivan, Aleyna
dc.contributor.authorPolat Korkunç, Ümmügülsüm
dc.contributor.authorBakırdere, Sezgin
dc.date.accessioned2023-10-18T10:46:17Z
dc.date.available2023-10-18T10:46:17Z
dc.date.issued2023en_US
dc.departmentFakülteler, Mühendislik ve Doğa Bilimleri Fakültesi, Kimya Mühendisliği Bölümüen_US
dc.description.abstractIn this study, a manganese ferrite (MnFe2O4) based dispersive solid phase extraction method (MF-DSPE) was proposed for the determination of lead (Pb) ions in hibiscus tea by double slotted quartz tube flame atomic absorption spectrometry (SQT-FAAS). The MnFe2O4 nanoparticles used as sorbent were produced in high yields using a green and friendly microwave synthesis procedure. The limit of detection (LOD) was found to be 14.2 µg/L under the optimal conditions. Recovery experiments were performed to assess the applicability of the developed method using hibiscus tea as test sample matrix. High recovery results were obtained by applying the matrix matching calibration method. Thanks to the developed MF-DSPE-SQT-FAAS method, the detection sensitivity for lead was improved by about 108-folds according to the comparison of the slopes of the calibration plots of the FAAS and MF-DSPE-SQT-FAAS systems.en_US
dc.identifier.citationKaraman, D. N., Serbest, H., Bahçivan, A., Polat Korkunç, Ü. & Bakırdere, S. (2023). Development of an analytical strategy for the determination of trace lead in hibiscus tea extract by double slotted quartz tube assisted flame atomic absorption spectrometry after manganese ferrite based dispersive solid phase extraction. Microchemical Journal, 195, pp. 1-8. https://doi.org/10.1016/j.microc.2023.109360en_US
dc.identifier.doi10.1016/j.microc.2023.109360en_US
dc.identifier.endpage8en_US
dc.identifier.issn1095-9149
dc.identifier.issn0026-265X
dc.identifier.scopus2-s2.0-85173246749en_US
dc.identifier.scopusqualityQ1en_US
dc.identifier.startpage1en_US
dc.identifier.urihttps://doi.org/10.1016/j.microc.2023.109360
dc.identifier.urihttps://hdl.handle.net/20.500.13055/562
dc.identifier.volume195en_US
dc.identifier.wosWOS:001091803100001en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.indekslendigikaynak.otherSCI-E - Science Citation Index Expandeden_US
dc.institutionauthorSerbest, Hakan
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofMicrochemical Journalen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.relation.tubitakinfo:eu-repo/grantAgreement/TUBITAK/SOBAG/1919B012209258
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDispersive Solid Phase Extractionen_US
dc.subjectFlame Atomic Absorption Spectrophotometryen_US
dc.subjectHibiscus Teaen_US
dc.subjectLeaden_US
dc.subjectMicrowave Synthesisen_US
dc.titleDevelopment of an analytical strategy for the determination of trace lead in hibiscus tea extract by double slotted quartz tube assisted flame atomic absorption spectrometry after manganese ferrite based dispersive solid phase extractionen_US
dc.typeArticleen_US
dspace.entity.typePublication

Dosyalar

Orijinal paket
Listeleniyor 1 - 1 / 1
Kapalı Erişim
İsim:
Development of an analytical strategy for the determination of trace lead in hibiscus tea extract by double slotted quartz tube assisted flame atomic abso.pdf
Boyut:
1.35 MB
Biçim:
Adobe Portable Document Format
Açıklama:
Tam Metin / Full Text
İndir
Lisans paketi
Listeleniyor 1 - 1 / 1
Kapalı Erişim
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Kimya Mühendisliği Bölümü Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu
WoS İndeksli Yayınlar Koleksiyonu